Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chlorophenyl chloroformate → 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chlorophenyl chloroformate | HCID 4184068 | — |
| 반응물 | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| 생성물 | 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate | HCID 57838891 | — |
반응 단계
2-(chloro)phenyl chloroformate (5.00 g, 26.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (4.50 g, 20.2 mmol) according to general procedure 1. Yield=4.56 g, 82%. m/z MH+=278.13. HPLC rt=9.3 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07888329B2 |
| 출처 데이터셋 | uspto-grants-2011_02 |
| ORD ID | ord-8b8bbe6a4ba54c138065b16c64258669 |
| 출처 메모 | uspto-grants-2011_02 |