Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → (2,5-Dimethoxyphenyl)acetyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 2,5-Dimethoxyphenylacetic acid | HCID 74469 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (2,5-Dimethoxyphenyl)acetyl chloride | HCID 596088 | — |
반응 단계
To a solution of 196 mg (1.00 mmol) of (2,5-dimethoxyphenyl)acetic acid in 3 mL of CH2Cl2 was added 100 μL of oxalyl chloride. The mixture was stirred at ambient temperature for 1 hour then concentrated under reduced pressure to a thick liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07888374B2 |
| 출처 데이터셋 | uspto-grants-2011_02 |
| ORD ID | ord-5f39d295ad2548daab8b070d6410a14a |
| 출처 메모 | uspto-grants-2011_02 |