Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate → 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate | HCID 24730367 | — |
| 반응물 | HCID 66940533 | HCID 66940533 | — |
| 생성물 | 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester | HCID 66940503 | 50% |
반응 단계
0.25 g (50% overall yield) of 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester was synthesized according to procedures described for the synthesis of 2-Amino-1H-benzoimidazole-4-carboxylic acid methyl ester (intermediate A) starting from 0.5 g (1.8 mmol) of above synthesized 2-Amino-3-nitro-5-pyridin-4-yl-benzoic acid methyl ester. LCMS: 269 (M+1)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07893267B2 |
| 출처 데이터셋 | uspto-grants-2011_02 |
| ORD ID | ord-94de602cfd914badaabf1906ea619415 |
| 출처 메모 | uspto-grants-2011_02 |