Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 6-Methyl-5-nitroquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 6-Methylquinoline | HCID 7059 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 6-Methyl-5-nitroquinoline | HCID 90009 | — |
반응 단계
2.45 mol of 6-methylquinoline were added to 1 l of concentrated sulfuric acid, and 2.94 mol of 65% strength nitric acid were added dropwise at 0 to 10° C. The mixture was stirred for 1 hour, poured onto ice, adjusted to pH 2.5 with aqueous sodium hydroxide solution, filtered off with suction, washed with water and dried over magnesium sulfate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06262074B1 |
| 출처 데이터셋 | uspto-grants-2001_07 |
| ORD ID | ord-fa9a47705e954ea291f0c63fe138790b |
| 출처 메모 | uspto-grants-2001_07 |