Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl 3-phenoxypropionate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 3-Phenoxypropionic acid | HCID 81596 | — |
| 촉매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Methyl 3-phenoxypropionate | HCID 347927 | 92.5% |
반응 단계
3-phenoxypropionic acid (5.0 g, 30 mmol) was dissolved in MeOH (12 mL) and H2SO4 (18 M, 3 drops) was added. The mixture was place in the microwave reactor (T: 140° C., t: 5 min). The solvent was evaporated, the mixture was partitioned in EtOAc (30 mL) and NaOH (2N, 20 mL). The organic phase was dried over MgSO4, filtered, and evaporated to give methyl 3-phenoxypropanoate (5.0 g, 27.7 mmol, 92.5%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08912177B2 |
| 출처 데이터셋 | uspto-grants-2014_12 |
| ORD ID | ord-f0e5c62721f74191816e661de8dbb9c6 |
| 출처 메모 | uspto-grants-2014_12 |