Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester | HCID 67201113 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 67199974 | HCID 67199974 | — |
반응 단계
(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester (10.8 g, 29.4 mmol) was dissolved in MeOH (70 mL) and purged with N2. Palladium on activated carbon (2.2 g, 10% by weight) was added, and the reaction mixture was charged with a balloon of H2. The reaction mixture was stirred for 3 h at room temperature, and then filtered through a pad of celite. The celite was washed with MeOH, and the filtrate was concentrated to afford 2.1 g (22%—two steps) of the sub-title compound. MS calculated for C17H27N3O4+H: 338, observed: 338.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07732618B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-6e5503b07a4e4e9296cb68f49fa4ee7f |
| 출처 메모 | uspto-grants-2010_06 |