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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 15575생성일: 2026년 10월 24일

(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974, 화합물

https://huagongshe.com/ko/reaction/15575

반응식

참여 물질

역할이름HCID투입량
반응물(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl esterHCID 67201113—
용매MethanolHCID 887—
생성물HCID 67199974HCID 67199974—

반응 단계

(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester (10.8 g, 29.4 mmol) was dissolved in MeOH (70 mL) and purged with N2. Palladium on activated carbon (2.2 g, 10% by weight) was added, and the reaction mixture was charged with a balloon of H2. The reaction mixture was stirred for 3 h at room temperature, and then filtered through a pad of celite. The celite was washed with MeOH, and the filtrate was concentrated to afford 2.1 g (22%—two steps) of the sub-title compound. MS calculated for C17H27N3O4+H: 338, observed: 338.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07732618B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-6e5503b07a4e4e9296cb68f49fa4ee7f
출처 메모uspto-grants-2010_06