Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178483770, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Phosphorus pentachloride | HCID 24819 | — |
| 반응물 | N,N-Dimethylethylenediamine | HCID 66053 | — |
| 반응물 | Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- | HCID 4712192 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 178483770 | HCID 178483770 | 42% |
반응 단계
Prepared as in Example 1 from 2-benzoyl-benzo[b]thiophen-3-ol, phosphorus(V) chloride and a solution of 2 parts by volume of N,N-dimethyl-ethylenediamine in 3 parts by volume of water with a yield of 42% of theory. Orange yellow crystals; m.p. 123°-125° C. (ethyl acetate).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04288437 |
| 출처 데이터셋 | uspto-grants-1981_09 |
| ORD ID | ord-4ebf388f804f408dbfd2a6de4d4f043c |
| 출처 메모 | uspto-grants-1981_09 |