Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-nitrophenol sodium salt → 1-Methoxy-4-[(4-nitrophenoxy)methyl]benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-nitrophenol sodium salt | HCID 13214 | — |
| 반응물 | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-Methoxy-4-[(4-nitrophenoxy)methyl]benzene | HCID 298745 | — |
반응 단계
To a solution of 24.2 g of sodium p-nitrophenoxide in 60 ml of DMF was added 23.5 g of 4-methoxybenzyl chloride. The precipitate was collected after 24 hours, washed with water, and recrystallized from chloroformcyclohexane, providing 1-methoxy-4-[(4-nitrophenoxy)methyl]benzene, mp 122°-124° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04555572 |
| 출처 데이터셋 | uspto-grants-1985_11 |
| ORD ID | ord-5f8c79e0d4354fa1b5878c551d3a58db |
| 출처 메모 | uspto-grants-1985_11 |