Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphorus oxychloride → 1-Allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphorus oxychloride | HCID 24813 | — |
| 반응물 | 2-Morpholinoaniline | HCID 735756 | — |
| 반응물 | 3-Allyl-1,1,3-trimethylurea | HCID 18952316 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine | HCID 15746402 | — |
반응 단계
Reaction of 3-allyl-1,1,3-trimethylurea (7.17 g) in benzene (50 ml) with 4-(2-aminophenyl)morpholine (6 g) in benzene (30 ml) in the presence of phosphorus oxychloride (4.71 ml) for 45 hours at 70° C. gave 1-allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine (bp. 148°-150° C. at 0.2 mm Hg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05223498 |
| 출처 데이터셋 | uspto-grants-1993_06 |
| ORD ID | ord-0a03cf096f38467fa596e0be8eb402a2 |
| 출처 메모 | uspto-grants-1993_06 |