Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Bis(benzyloxy)trimethylamine → HCID 178484264, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Bis(benzyloxy)trimethylamine | HCID 74837 | — |
| 반응물 | HCID 178509386 | HCID 178509386 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 178484264 | HCID 178484264 | — |
반응 단계
In 1 ml of toluene, 57.3 mg (0.25 mmol) of 5-amino-3-(4-nitro-phenyl)-1H-pyrazole-4-carbonitrile and 79.3 μl of N,N-dimethylformamide dibenzylacetal are boiled overnight. Filtering of the suspension and washing with hexane yield N'-[3-(4-nitro-phenyl)-4-cyano-1H-pyrazol-5-yl]-N,N-dimethylformamidine; TLC: Rf =0.15 (ethyl acetate:hexane=2:1); TRet (Grad20-100)=8.8.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05981533 |
| 출처 데이터셋 | uspto-grants-1999_11 |
| ORD ID | ord-d4a79f1b57114cb8b3706a09b566e770 |
| 출처 메모 | uspto-grants-1999_11 |