Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichloropyrazine → HCID 59343416, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichloropyrazine | HCID 78504 | — |
| 반응물 | 4-Hydroxy-1-indanone | HCID 590547 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 59343416 | HCID 59343416 | 90% |
반응 단계
Using Method DD with 2,6-dichloropyrazine (200 mg, 1.34 mmol) and 4-hydroxyindanone (219 mg, 1.49 mmol), and crystallisation in AcOEt, the title compound was obtained (314 mg). Yield: 90%. 1H NMR (250 MHz, DMSO-d6) δ 2.70 (t, 2H, H3, J=5.7 Hz), 2.94 (t, 2H, H2, J=5.7 Hz), 7.55-7.64 (m, 3H, Harom), 8.57 (s, 1H, HPz 5), 8.66 (s, 1H, HPz 3). m/z: 261.0 [(M+H)+, calcd for C13H9ClN2O2 260.0].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737152B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-af2b4878a7334a5696155266686bb51d |
| 출처 메모 | uspto-grants-2010_06 |