Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
10-Undecenal → N-[(E)-undec-10-enylideneamino]benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 10-Undecenal | HCID 8187 | — |
| 반응물 | Benzoylhydrazine | HCID 11955 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-[(E)-undec-10-enylideneamino]benzamide | HCID 87145928 | 88.2% |
반응 단계
A mixture of 1a (1.50 g, 11.0 mmol) and 10-undecenal (2.80 g, 16.5 mmol) in ethanol (28 ml) was heated under reflux for 2 h. After cooling to room temperature, the product was concentrated, washed with hexane and dried under vacuum (0.20 mbar) to give 2.78 g (88%) of a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08124578B2 |
| 출처 데이터셋 | uspto-grants-2012_02 |
| ORD ID | ord-aee1b8b35d8749a7b1ff9995fd7ce5cf |
| 출처 메모 | uspto-grants-2012_02 |