반응식
F[CH:2](F)[C:3](O)([C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[CH3:10])C(F)(F)F.CC(=O)C(=O)CC>>[F:11][C:9]([F:12])([C:8]([F:14])([F:13])[CH2:3][CH3:2])[CH3:10]참가 물질
실험 절차
As another example, 2-difluoromethyl-1,1,1,3,3,4,4-heptafluoro-2-pentanol may be prepared by fluorinating commercially available 2,3-pentanedione to form 2,2,3,3-tetrafluoropentane which may then be dehydrogenated to form 3,3,4,4-tetrafluoro-1-pentene. CF3 may then be added to the 3,3,4,4-tetrafluoro-1-pentene to form 2-trifluoromethyl-1,3,3,4,4-pentafluoropentane which may then be dehydrogenated to form 2-trifluoromethyl-1,3,3,4,4-pentafluoro-1-pentene. The 2-trifluoromethyl-1,3,3,4,4-pentafluoro-1-pentene may then be reacted with hydrogen fluoride to form 2-trifluoromethyl-1,1,3,3,4,4-hexafluoropentane which may then be dehydrogenated to form 2-trifluoromethyl-1,1,3,3,4,4-hexafluoro-1-pentene which may then be reacted with sulfuric acid and then water to form 2-difluoromethyl-1,1,1,3,3,4,4-heptafluoro-2-pentanol.
출처 및 근거
- ORD 기록
- ord-a84660bd1da0410ea3723bd866eba1ab
- 출처 데이터셋
- uspto-grants-1993_10
- 특허 번호
- US05254755
연결된 노트
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