Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Carbonate → Dimethyldidecyl ammonium methylcarbonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Carbonate | HCID 12021 | — |
| 반응물 | 1-Decanamine, N-decyl-N-methyl- | HCID 81880 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Dimethyldidecyl ammonium methylcarbonate | HCID 86632012 | — |
반응 단계
Into an autoclave equipped with a stirrer, didecylmethylamine (1 mol), dimethylcarbonate (1.5 mol) and methanol (2.0 mol) as a solvent were introduced, and a reaction was carried out at a reaction temperature of 110° C. for 12 hours to obtain a methanol solution of dimethyldidecyl ammonium methylcarbonate. To this solution, octylic acid (1 mol) was added, and by removing carbon dioxide and methanol, which were formed as byproducts, dimethyl didecylammonium/octylate (quaternary ammonium salt (B1)) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08030428B2 |
| 출처 데이터셋 | uspto-grants-2011_10 |
| ORD ID | ord-540301ad4e1c444c88ffeed1f330ab19 |
| 출처 메모 | uspto-grants-2011_10 |