Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl (2e)-3-[4-amino-3-(4-phenoxyphenyl)thieno[3,2-c]pyridin-7-yl]acrylate → (2e)-3-[4-Amino-3-(4-phenoxyphenyl)thieno[3,2-c]pyridin-7-yl]acrylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl (2e)-3-[4-amino-3-(4-phenoxyphenyl)thieno[3,2-c]pyridin-7-yl]acrylate | HCID 69776505 | — |
| 용매 | Trifluoroacetic acid | HCID 6422 | — |
| 생성물 | (2e)-3-[4-Amino-3-(4-phenoxyphenyl)thieno[3,2-c]pyridin-7-yl]acrylic acid | HCID 18450609 | — |
반응 단계
A solution of Example 11A (0.25 g, 0.57 mmol) in TFA (5 mL) was stirred at room temperature for 14 hours then concentrated under a stream of nitrogen to provide the desired product. MS (ESI(+)) m/e 388.9 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737160B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-41b775617d9b4016b5738eb1a013ed0c |
| 출처 메모 | uspto-grants-2010_06 |