Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Heptanedione → 2-[3-(4-Chlorophenoxy)propyl]-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Heptanedione | HCID 81923 | — |
| 반응물 | HCID 178508402 | HCID 178508402 | — |
| 생성물 | 2-[3-(4-Chlorophenoxy)propyl]-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 76684687 | 44% |
반응 단계
The title compound was prepared according to the experimentals described for Example 22 above from 3-[3-(4-chlorophenoxy)propyl]-1H-1,2,4-triazol-5-amine and 3,5-heptanedione in 44% yield; 1H NMR (DMSO-d6, 400 MHz) δ ppm: 7.31 (dd, 1H), 7.29 (dd, 1H), 7.11 (s, 1H), 6.96 (dd, 1H), 6.94 (dd, 1H), 4.08 (t, 2H), 3.07 (q, 2H), 2.97 (t, 2H), 2.86 (q, 2H), 2.20 (m, 2H), 1.33 (t, 3H), 1.27 (t, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09163027B2 |
| 출처 데이터셋 | uspto-grants-2015_10 |
| ORD ID | ord-05c243ae70324d5ebc86776090fa9e8d |
| 출처 메모 | uspto-grants-2015_10 |