Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene, (3-chloro-1-propenyl)- → 6-Phenyl-5-hexen-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene, (3-chloro-1-propenyl)- | HCID 94242 | — |
| 반응물 | 5-Methyl-5-hexen-2-one | HCID 228604 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 6-Phenyl-5-hexen-2-one | HCID 53812467 | — |
반응 단계
The synthesis was similar to that used for 5-methyl-5-hexen-2-one. Materials that were used: cinnamyl chloride (100 g, 0.655 mole, Acros Organic), pentadione (72 g, 0.72 mole), and ethanol (460 mL). Product, 70-75° C., 0.1 mmHg, 48 g (42%). 1H-NMR (CDCl3, δ): 2.15 (s, 3H); 2.16 (m, 2H); 2.60 (m, 2H); 6.17 (m, 1H), 6.42 (d, 1H), 7.2-7.33 (m, 5H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741375B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-a2dda68f11c4401d839282a53a343e21 |
| 출처 메모 | uspto-grants-2010_06 |