Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dichloro-4-isocyanatopyridine → N-(2,6-Dichloropyridin-4-yl)-2-(4,8-dimethylquinolin-2-yl)hydrazinecarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dichloro-4-isocyanatopyridine | HCID 2781658 | — |
| 반응물 | 2-Hydrazinyl-4,8-dimethylquinoline | HCID 3684316 | — |
| 생성물 | N-(2,6-Dichloropyridin-4-yl)-2-(4,8-dimethylquinolin-2-yl)hydrazinecarboxamide | HCID 52912060 | — |
반응 단계
A solution of 2-hydrazinyl-4,8-dimethylquinoline (110 mg, 0.60 mmol) and 111 mg (1.0 eq) of 2,6-dichloro-4-isocyanatopyridine was reacted as outlined in Scheme 1 above to give the desired title compound. Spectroscopic data: 1H NMR (300 MHz, DMSO-d6) δ ppm 2.50 (s, 3 H) 2.56 (s, 3 H) 6.79 (s, 1 H) 7.18 (t, J=7.62 Hz, 1 H) 7.41 (d, J=7.03 Hz, 1 H) 7.70 (d, J=8.20 Hz, 2 H) 8.72 (s, 2 H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08507682B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-14dc0746e03a4f76b610f4fee0d3a823 |
| 출처 메모 | uspto-grants-2013_08 |