Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl 4-oxopiperidine-1-carboxylate → tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| 반응물 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
| 생성물 | tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate | HCID 59333733 | 48% |
반응 단계
tert-Butyl 3-(3-(3-fluorophenyl)propanoyl)-4-oxopiperidine-1-carboxylate (285 mg, 48%) was synthesised from tert-butyl 4-oxopiperidine-1-carboxylate and 3-(3-fluorophenyl)propanoyl chloride according to the general procedure for the preparation of diketones. MS (ES+) m/z 250 (M+H)+
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08188101B2 |
| 출처 데이터셋 | uspto-grants-2012_05 |
| ORD ID | ord-41125c7fb85541a8968bc3f605dc388a |
| 출처 메모 | uspto-grants-2012_05 |