Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl tryptophanate hydrochloride → N-(3,5-dimethylbenzoyl)-N-methyl-O-methyl-(D)-tyrosyl-(L)-tryptophan
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl tryptophanate hydrochloride | HCID 2734891 | — |
| 반응물 | N-(3,5-dimethylbenzoyl)-N-methyl-(D)-tyrosyl-(L)-tryptophan | HCID 67675232 | — |
| 생성물 | N-(3,5-dimethylbenzoyl)-N-methyl-O-methyl-(D)-tyrosyl-(L)-tryptophan | HCID 67674645 | — |
반응 단계
Coupling of N-(3,5-dimethylbenzoyl)-N-methyl-O-methyl-(D)-tyrosine (prepared by O-methylation of N-(3,5-dimethylbenzoyl)-N-methyl-(D)-tyrosine (example 64)) with (L)-tryptophan methyl ester hydrochloride according to example 1 followed by hydrolysis of the methyl ester moiety according to example 12 gives N-(3,5-dimethylbenzoyl)-N-methyl-O-methyl-(D)-tyrosyl-(L)-tryptophan; FAB-MS m/e 528 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05780498 |
| 출처 데이터셋 | uspto-grants-1998_07 |
| ORD ID | ord-72ef96e7591149e7b1f9a21c90168308 |
| 출처 메모 | uspto-grants-1998_07 |