Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Succinic anhydride → Irgacure 2959 monosuccinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Succinic anhydride | HCID 7922 | — |
| 반응물 | 2-Hydroxy-1-(4-(hydroxyethoxy)phenyl)-2-methyl-1-propanone | HCID 86266 | — |
| 생성물 | Irgacure 2959 monosuccinate | HCID 131730535 | — |
반응 단계
As an illustrative example, a tri-functional compound can be prepared as follows. Irgacure 2959 (4-(2-hydroxyethoxy)phenyl-(2-hydroxy-2-propyl)ketone) can be reacted with succinic anhydride (reflux in triethylamine/Toluene) to obtain Irgacure 2959-monosuccinate. Norbloc (2-{3-(2H-Benxotriazol-2-yl)-4-hydroxyphenyl}ethyl methacrylate) is reacted with the obtained Irgacure 2959-monosuccinate in the presence of N,N-dicyclohexyl carbodiimide (DCC) and 4-(dimethylamino)pyridine (D-MAP) to obtain conjugated Irgacure 2959-Norbloc.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08431624B2 |
| 출처 데이터셋 | uspto-grants-2013_04 |
| ORD ID | ord-3bd98ddf18f84b69902ca67453ad2153 |
| 출처 메모 | uspto-grants-2013_04 |