Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromopropane → alpha-Isopropyl-3,5-dimethoxyphenylacetonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromopropane | HCID 6358 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3,5-Dimethoxyphenylacetonitrile | HCID 139445 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | alpha-Isopropyl-3,5-dimethoxyphenylacetonitrile | HCID 14183624 | — |
반응 단계
This is prepared by reacting a solution of 2-(3,5-dimethoxyphenyl)-acetonitrile (4 g, 0.022 mol) in 10 cc of DMF with 2.86 g of isopropyl bromide in 5 cc of DMF, in the presence of a 50% suspension of 1.1 g of sodium hydride in 25 cc of DMF.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04481207 |
| 출처 데이터셋 | uspto-grants-1984_11 |
| ORD ID | ord-d047fe9f29f94682b2e0ae160cb0a8d9 |
| 출처 메모 | uspto-grants-1984_11 |