참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chloroethanol | HCID 34 | — |
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Trifluoromethanesulfonic anhydride | HCID 67749 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 2-Chloroethyl trifluoromethanesulfonate | HCID 100525 | — |
반응 단계
A solution of triflic anhydride (2.0 mL, 11.9 mmol) in CCl4 (10 mL) at 0° C. was treated with a solution of 2-chloroethanol (0.8 mL, 11.9 mmol) and pyridine (0.96 mL, 11.9 mmol) in CCl4 (6.0 mL) which was pre-cooled to 0° C. The reaction mixture was stirred at 0° C. for 45 minutes and then filtered through a pad of Na2SO4. The filtrate was concentrated and used immediately in the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07514435B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_04 |
|---|
| ORD ID | ord-34b7e7b7c1094e9f844c0b8f5b74f1fb |
|---|
| 출처 메모 | uspto-grants-2009_04 |
|---|
