참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acrylamide | HCID 6579 | — |
| 반응물 | tert-Butyl acrylate | HCID 15458 | — |
| 반응물 | Ethanaminium, N,N,N-trimethyl-2-[(1-oxo-2-propen-1-yl)oxy]-, chloride (1:1) | HCID 162071 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | t-Butylacrylate Acrylamide | HCID 86584091 | — |
반응 단계
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammonioethylacrylate chloride, 8.06 g of t-butylacrylate, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ˜15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06692732B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_02 |
|---|
| ORD ID | ord-64b0f2c210b245d8a93de1ea01f1fbe3 |
|---|
| 출처 메모 | uspto-grants-2004_02 |
|---|
