참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Cyanide | HCID 8929 | — |
| 반응물 | Trivinyl(3-chloropropyl)silane | HCID 23630656 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Cyanopropyltrivinylsilane | HCID 57945605 | 86.2% |
반응 단계
Compound 3-chloropropyltrivinylsilane (1000 mg, 5.35 mmol) and sodium cyanide (525 mg, 10.70 mmol) were dissolved in 18 ml of dimethylformamide, and the mixture was heated at 70° C. for 4 hours. After the reaction, the organic layer was extracted after addition of distilled water and ether, and then purified by column chromatography (n-Hex:EA=10:1, Rf=0.42), to give 818 mg (86% yield) of pure 3-cyanopropyltrivinylsilane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08197903B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_06 |
|---|
| ORD ID | ord-6de4cb8820464af5bd48ac5f26ac22a1 |
|---|
| 출처 메모 | uspto-grants-2012_06 |
|---|
