Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Azido-2-[2-(2-azidoethoxy)ethoxy]ethane → Bis-Aminoethylglycol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Azido-2-[2-(2-azidoethoxy)ethoxy]ethane | HCID 10845705 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Bis-Aminoethylglycol | HCID 70248 | — |
반응 단계
To a solution of diazide 19 (14.67 g, 0.073 mol) in THF (100 ml) 1.5 g of 5% Pt on charcoal is added. The mixture is stirred for 12 h under hydrogen. Filtration through Celite™ and evaporation of solvents at reduced pressure gives 1,8-diamino-3,6-dioxa-octane 20.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06399071B1 |
| 출처 데이터셋 | uspto-grants-2002_06 |
| ORD ID | ord-a477a5d3ee1340b9ac5c6b429b66c7c0 |
| 출처 메모 | uspto-grants-2002_06 |