반응식
O[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9].[CH2:10]([SH:12])[CH3:11]>>[CH2:10]([S:12][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])[CH3:11]참가 물질
3
실험 절차
A mixture of 49.6 g (0.4 mol) of 2-hydroxymethyl-phenol and 124 g (2 mol) of ethylmercaptan was heated for 5 hours to 170° C. in a stirred autoclave. Working up as in Example 1 gave 32.2 g (96% of theory) of 2-ethylthiomethyl-phenol.
후처리
- temperaturewas heated for 5 hours to 170° C. in a stirred autoclave
출처 및 근거
- ORD 기록
- ord-eacb17e009e84059b307f1326fc1641a
- 출처 데이터셋
- uspto-grants-1982_11
- 특허 번호
- US04358616
연결된 노트
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