참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | O-Phenylenediamine | HCID 7243 | — |
| 반응물 | Isatoic Anhydride | HCID 8359 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Benzo[b][1,4]benzodiazepin-6-one | HCID 19781529 | 96% |
반응 단계
A mixture of isatoic anhydride (1 mol) and 1,2 phenylenediamine (1.1 mol) in aglacial acetic acid (60%) was heated at 75° C. for 3 hrs. The resulting mixture was diluted with water and solid filtered to obtained dibenzo[b,e][1,4]-diazepine-11-one in 96% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08202989B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_06 |
|---|
| ORD ID | ord-2936c68d6a464830925ee60bd4de99dd |
|---|
| 출처 메모 | uspto-grants-2012_06 |
|---|
