Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Trifluoromethyl)benzoyl chloride → ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
| 반응물 | Ethyl 4-chloro-2-fluorobenzimidate | HCID 19373098 | — |
| 생성물 | ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate | HCID 21283811 | — |
반응 단계
starting from ethyl 4-chloro-2-fluorobenzimidate and o-trifluoromethyl-benzoyl chloride there is obtained ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate and therefrom with methylhydrazine there is obtained 3-(4-chloro-2-fluorophenyl)-1-methyl-5-(o-trifluoromethyl-phenyl)-1H-1,2,4-triazole, m.p. 109.5°-112° C.;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04788210 |
| 출처 데이터셋 | uspto-grants-1988_11 |
| ORD ID | ord-3daaab40184244b4bb87d50d9da2fd6c |
| 출처 메모 | uspto-grants-1988_11 |