Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxygen → Carboxyphenylstearic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxygen | HCID 977 | — |
| 반응물 | Methyl Ethyl Ketone | HCID 6569 | — |
| 반응물 | Butane | HCID 7843 | — |
| 반응물 | 2-(2-Methylphenyl)octadecanoic acid | HCID 22323937 | — |
| 촉매 | Cobalt diacetate | HCID 6277 | — |
| 생성물 | Carboxyphenylstearic acid | HCID 70555697 | 47.9% |
반응 단계
The oxidation procedure of Example I was repeated except that only 40 gms cobalt (II) acetate was employed. Also, for this reaction 40 gms methylethyl ketone and 72 gms butane were charged to the reactor. Eighty percent conversion of the tolylstearic acid was achieved after only four hours reaction (105° C. and 350 psig O2). Carboxyphenylstearic acid was obtained in 47.9% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04356315 |
| 출처 데이터셋 | uspto-grants-1982_10 |
| ORD ID | ord-0445cac1340449bb900981407bee45ad |
| 출처 메모 | uspto-grants-1982_10 |