참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | GlyTouCan:G36918VO | HCID 439559 | — |
| 촉매 | Nickel | HCID 935 | — |
| 생성물 | Isomaltitol | HCID 94169 | 49.7% |
반응 단계
In accordance with the process described in Example 1, 7.5 kg isomaltulose were dissolved at 80° C. to form a 75% by weight aqueous solution and then transferred to a heated autoclave equipped with an agitator and having a capacity of 20 l. In the autoclave the solution was mixed with an aqueous catalyst suspension containing 500 g Raney nickel. Hydrogenation and crystallization were then carried out as described in Example 1. After a reaction period of 3 hours, the isomaltulose charge had been hydrogenated to form 3.75 kg each of isomaltitol and glucopyranosido-1,6-mannitol. 3.45 kg isomaltitol and 3.45 kg glucopyranosido-1,6-mannitol could then be obtained therefrom in crystal form by means of the fractional crystallization operation described in Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04233439 |
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| 출처 데이터셋 | uspto-grants-1980_11 |
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| ORD ID | ord-2f1ff2bf9e5d4602b04609c424645ef2 |
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| 출처 메모 | uspto-grants-1980_11 |
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