Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,5-Bis(trifluoromethyl)aniline → 2-[4'-Chloro-5-(2,5-bis-trifluoromethyl-phenylamino)-3'-trifluoromethyl-biphenyl-3-yl]-4-methyl-pentanoic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,5-Bis(trifluoromethyl)aniline | HCID 719818 | — |
| 반응물 | 2-(4'-Chloro-5-trifluoromethanesulfonyloxy-3'-trifluoromethyl-biphenyl-3-yl)-4-methyl-pentanoic acid methyl ester | HCID 57754964 | — |
| 생성물 | 2-[4'-Chloro-5-(2,5-bis-trifluoromethyl-phenylamino)-3'-trifluoromethyl-biphenyl-3-yl]-4-methyl-pentanoic acid methyl ester | HCID 57755009 | 35% |
반응 단계
The title compound was prepared in 35% yield from 2-(4′-chloro-5-trifluoromethanesulfonyloxy-3′-trifluoromethyl-biphenyl-3-yl)-4-methyl-pentanoic acid methyl ester and 2,5-bis-(trifluoromethyl)aniline under the conditions described in Example 37, step (b).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07557244B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-5d07c72995b346bf8a9c72bffe1a1a15 |
| 출처 메모 | uspto-grants-2009_07 |