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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2276621생성일: 2026년 10월 24일

Bromobenzene → 1-Pentadecyl-3-phenoxybenzene

https://huagongshe.com/ko/reaction/2276621

반응식

참여 물질

역할이름HCID투입량
반응물BromobenzeneHCID 7961—
반응물DimethylacetamideHCID 31374—
반응물Hydrogenated cardanolHCID 68146—
반응물PotassiumHCID 5462222—
용매WaterHCID 962—
생성물1-Pentadecyl-3-phenoxybenzeneHCID 17747909—

반응 조건

온도150 °C

반응 단계

Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09133089B2
출처 데이터셋uspto-grants-2015_09
ORD IDord-098d7520d0d44e888b6a85333b30fb9f
출처 메모uspto-grants-2015_09