Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dimethoxybenzaldehyde → [8-Benzyloxy-2-(3,5-dimethoxyphenyl)-imidazo[1,2-a]pyridin-3-ylamino]-acetic acid methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dimethoxybenzaldehyde | HCID 81747 | — |
| 반응물 | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| 반응물 | Methyl isocyanoacetate | HCID 547815 | — |
| 용매 | Perchloric Acid | HCID 24247 | — |
| 생성물 | [8-Benzyloxy-2-(3,5-dimethoxyphenyl)-imidazo[1,2-a]pyridin-3-ylamino]-acetic acid methyl ester | HCID 69731334 | — |
반응 단계
Compound (9) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of methyl isocyanoacetate solution (0.2 M, DCM), 0.500 ml of 3,5-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849642B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-c1a9efe4ec324f5ca9ac07f17e534daa |
| 출처 메모 | uspto-grants-2005_02 |