Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexyl isocyanate → HCID 178418561, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexyl isocyanate | HCID 75659 | — |
| 반응물 | 3-[4-(4-Chlorobenzyl)homopiperazin-1-yl]-propanethiol | HCID 20153174 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178418561 | HCID 178418561 | 77.6% |
반응 단계
The procedure described in Example 2 was followed, using 1.3 g of n-hexyl isocyanate, 3.0 g of 3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propanethiol and 75 ml of methylene chloride, to give 1.3 g (33% of theory) of N-(n-hexyl)-S-{3-[4-(4-chlorobenzyl)homopiperazin-1-yl]propyl}thiocarbamate dihydrochloride as a tan powder, M.p. 183°-187° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04618677 |
| 출처 데이터셋 | uspto-grants-1986_10 |
| ORD ID | ord-997e1d6449954340b4d905cb9ec92291 |
| 출처 메모 | uspto-grants-1986_10 |