Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 반응물 | 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde | HCID 21474525 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanol | HCID 21474532 | — |
반응 단계
1.6 g (5 mmol) of the aldehyde obtained in Example 45, 50 ml of THF and 50 ml of methanol are introduced into a round-bottomed flask. 100 mg (2.5 mmol) of sodium borohydride are added in small portions and the mixture is stirred at room temperature for 4 h. The reaction medium is poured into water, the mixture is extracted with ethyl ether and the organic phase is separated after settling has taken place, dried over magnesium sulphate and evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05688817 |
| 출처 데이터셋 | uspto-grants-1997_11 |
| ORD ID | ord-9042ac85129e49f6a5842e3c018e510b |
| 출처 메모 | uspto-grants-1997_11 |