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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2294582생성일: 2026년 10월 24일

Methanol → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanol

https://huagongshe.com/ko/reaction/2294582

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물TetrahydrofuranHCID 8028—
반응물Sodium borohydrideHCID 4311764—
반응물4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehydeHCID 21474525—
용매WaterHCID 962—
생성물4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzenemethanolHCID 21474532—

반응 단계

1.6 g (5 mmol) of the aldehyde obtained in Example 45, 50 ml of THF and 50 ml of methanol are introduced into a round-bottomed flask. 100 mg (2.5 mmol) of sodium borohydride are added in small portions and the mixture is stirred at room temperature for 4 h. The reaction medium is poured into water, the mixture is extracted with ethyl ether and the organic phase is separated after settling has taken place, dried over magnesium sulphate and evaporated.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05688817
출처 데이터셋uspto-grants-1997_11
ORD IDord-9042ac85129e49f6a5842e3c018e510b
출처 메모uspto-grants-1997_11