Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 3-Bromo-1,2-propanediol | HCID 20827 | — |
| 반응물 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 생성물 | 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane | HCID 169759 | — |
반응 단계
An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04851502 |
| 출처 데이터셋 | uspto-grants-1989_07 |
| ORD ID | ord-137e2323cbb8440bab45f00bb57fe83c |
| 출처 메모 | uspto-grants-1989_07 |