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HRID 234071생성일: 2026년 10월 24일

1,3-Bis(4-methylphenyl)prop-2-en-1-one → 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene

https://huagongshe.com/ko/reaction/234071

반응식

참여 물질

역할이름HCID투입량
반응물1,3-Bis(4-methylphenyl)prop-2-en-1-oneHCID 256552—
촉매PalladiumHCID 23938—
용매Acetic AcidHCID 176—
생성물1-Methyl-4-[3-(4-methylphenyl)propyl]benzeneHCID 57172699.4%

반응 단계

To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05594081
출처 데이터셋uspto-grants-1997_01
ORD IDord-9c59153766d74092b67b123096222700
출처 메모uspto-grants-1997_01