Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Bis(4-methylphenyl)prop-2-en-1-one → 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Bis(4-methylphenyl)prop-2-en-1-one | HCID 256552 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene | HCID 571726 | 99.4% |
반응 단계
To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05594081 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-9c59153766d74092b67b123096222700 |
| 출처 메모 | uspto-grants-1997_01 |