Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Monochloramine → Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Monochloramine | HCID 25423 | — |
| 반응물 | alpha,2,6-Trimethylmorpholin-4-ylethanol | HCID 98999 | — |
| 생성물 | Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) | HCID 77210 | — |
반응 단계
An amount, 398.5 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.3 moles) was condensed with the free chloroamine obtained from 390.5 grams N-chloroethyl morpholine hydrochloride (2.3 moles) as described above to give 325.4 grams (55.7%) of the catalyst as a pale yellow oil, bp 122°-124° C. at 0.3 mm of Hg. The structure was confirmed by elemental analysis, calc. 62.9 C, 10.6 H, 9.8 N; found 62.2 C, 10.4 H, 9.8 N.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04871845 |
| 출처 데이터셋 | uspto-grants-1989_10 |
| ORD ID | ord-b73797ea32e046c1b7817753ec89f853 |
| 출처 메모 | uspto-grants-1989_10 |