Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Methoxide → 3-cyanophenyl 5-thio-beta-D-xylopyranoside
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 반응물 | 3-cyanophenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 15067856 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-cyanophenyl 5-thio-beta-D-xylopyranoside | HCID 15067857 | 85% |
반응 단계
If the procedure described in Preparation LXXXIV is followed starting from 2.12 g (5.4.10-3 mol) of 3-cyanophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside and 0.2 ml of a solution of sodium methylate in methanol (8% w/v of Na), reacted in 60 ml of methanol for 30 min, 1.22 g (yield: 85%) of the expected product are obtained after precipitation in ether and lyophilization.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05101048 |
| 출처 데이터셋 | uspto-grants-1992_03 |
| ORD ID | ord-03ffb509e26948c681847be72f92c18d |
| 출처 메모 | uspto-grants-1992_03 |