Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → HCID 86638666, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | O-(2,4-dinitrophenyl)hydroxylamine | HCID 87140 | — |
| 반응물 | 2H,3H-furo(3,2-c)pyridine | HCID 15534896 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 86638666 | HCID 86638666 | 89% |
반응 단계
To a solution of 2,3-dihydrofuro[3,2-c]pyridine (23.8 g, 200 mmol) in acetonitrile (130 mL) was added 1-(aminooxy)-2,4-dinitrobenzene (55.0 g, 240 mmol), and the mixture was stirred at room temperature for 3 days. Diethyl ether was added, and the resulting precipitate was collected by filtration to give the title compound (57.0 g, yield 89%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08273761B2 |
| 출처 데이터셋 | uspto-grants-2012_09 |
| ORD ID | ord-3803696f5b5b41f78877e96682917329 |
| 출처 메모 | uspto-grants-2012_09 |