Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetaldehyde, 2,2-dimethoxy- → N-(2,2-dimethoxyethyl)-4-fluoro-3-methoxyaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetaldehyde, 2,2-dimethoxy- | HCID 162650 | — |
| 반응물 | 4-Fluoro-3-methoxyaniline | HCID 2774533 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-(2,2-dimethoxyethyl)-4-fluoro-3-methoxyaniline | HCID 22570019 | 101.1% |
반응 단계
To a solution of 4-fluoro-3-methoxyaniline (0.98 g 6.9 mmol) in ethanol (20 ml) was added glyoxal 1,1-dimethyl acetal (0.89 g 8.27 mmol). Pd/C 5% (50 mg) was added and the mixture hydrogenated. Removal of the catalyst by filtration and evaporation of solvent in vacuo gave N-(2,2-dimethoxyethyl)-4-fluoro-3-methoxyaniline 1.6 g
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06855715B1 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-a5bf9884b51f40babe1c53423ffc7dc7 |
| 출처 메모 | uspto-grants-2005_02 |