Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4,5-Trimethoxybenzoyl chloride → Benzamide, N-(1,2,3,4-tetrahydro-2-methylisoquinolin-5-yl)-2,4,5-trimethoxy-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4,5-Trimethoxybenzoyl chloride | HCID 2760809 | — |
| 반응물 | 2-Methyl-1,2,3,4-tetrahydroisoquinolin-5-amine | HCID 14171269 | — |
| 생성물 | Benzamide, N-(1,2,3,4-tetrahydro-2-methylisoquinolin-5-yl)-2,4,5-trimethoxy- | HCID 216596 | — |
반응 단계
5-Amino-2-methyl-1,2,3,4-tetrahydroisoquinoline was reacted with 2,4,5-trimethoxybenzoyl chloride according to the procedure of Example 19 to yield 5-(2,4,5-trimethoxybenzamido)-2-methyl-1,2,3,4-tetrahydroisoquinoline; m.p. 159°-160.5° C. after purification from ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04022900 |
| 출처 데이터셋 | uspto-grants-1977_05 |
| ORD ID | ord-ecbe45762ab840158cd1cbf6233030f3 |
| 출처 메모 | uspto-grants-1977_05 |