Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol → Phenyl 4-methylpentanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Pentanoyl chloride, 4-methyl- | HCID 170008 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Phenyl 4-methylpentanoate | HCID 12653656 | 88% |
반응 단계
4-Methylpentanoyl chloride (3.0 g, 22.3 mmol) was added dropwise to phenol (2.1 g, 22.3 mmol). After 3 hours, H2O was added and the reaction mixture was extracted with Et2O. The organic phase was washed with NaHCO3, then brine to neutrality, then dried (Na2SO4), concentrated and bulb-to-bulb distilled to afford the title compound in 88% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08648032B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-2fdca11ac0de4538881cd3f7ef310dc2 |
| 출처 메모 | uspto-grants-2014_02 |