참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzyl azide | HCID 12152 | — |
| 반응물 | Tributyl(2-phenylethynyl)stannane | HCID 630640 | — |
| 생성물 | HCID 68738217 | HCID 68738217 | — |
반응 단계
Phenylethynyltri-n-butyltin (8.25 g, 21.1 mmol) and benzyl azide (2.3 mL, 18.4 mmol) were combined and heated to 150° C. overnight. The mixture was purified by silica gel chromatography eluting with a gradient of 5-40% ethyl acetate in hexanes to afford the title compound. MS (ESI+) m/z 526.3 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08648069B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-188aec90da8d407986ced84dd7f2e5c8 |
|---|
| 출처 메모 | uspto-grants-2014_02 |
|---|
