참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzyl azide | HCID 12152 | — |
| 반응물 | Tributyl(prop-1-yn-1-yl)stannane | HCID 2733165 | — |
| 생성물 | 1-Benzyl-5-methyl-4-(tributylstannyl)-1H-1,2,3-triazole | HCID 68990342 | — |
반응 단계
Tributyl(1-propynyl)tin (3.87 g, 11.8 mmol) and benzyl azide (2.2 mL, 17.6 mmol) were combined and heated to 150° C. overnight. The mixture was purified by silica gel chromatography eluting with a gradient of 5-40% ethyl acetate in hexanes to afford the title compound. MS (ESI+) m/z 464.2 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08648069B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-b4ca326d8b7d43b6a5b90edc7a946609 |
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| 출처 메모 | uspto-grants-2014_02 |
|---|
