Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propynamide → 2-[4-(Aminocarbonyl)-1H-1,2,3-triazol-1-yl]propanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propynamide | HCID 101445 | — |
| 반응물 | Tert-butyl 2-azidopropanate | HCID 86634922 | — |
| 생성물 | 2-[4-(Aminocarbonyl)-1H-1,2,3-triazol-1-yl]propanoic acid | HCID 57907639 | — |
반응 단계
2-[4-(Aminocarbonyl)-1H-1,2,3-triazol-1-yl]propanoic acid was prepared from commercially available propiolamide and tert-butyl 2-azidopropanate using a procedure analogous to that used to prepare Intermediate 52. 1HNMR (500 MHz, CD3OD) δ: 8.48 (s, 1H), 5.50 (q, J=7.3 Hz, 1H), 1.85 (d, J=7.3 Hz, 3H). LC-MS: m/z (ES) 185 (MH)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08653260B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-a12b8c610eee4f409f9c783861cd25c0 |
| 출처 메모 | uspto-grants-2014_02 |