Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 4-Propyl-1,2-benzenediol | HCID 97638 | — |
| 반응물 | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol | HCID 15165616 | — |
반응 단계
The same procedures as described in Example 10 were carried out by using a mixture of 7.61 g (50 mM) of 4-n-propylcatechol, 15 ml of acetone, 30 mg of p-toluenesulfonic acid monohydrate and 15 ml of benzene. 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol was obtained in the yield of 9.13 g (47 mM) as colorless transparent liquid having a boiling point of 82°-87° C./3 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05214034 |
| 출처 데이터셋 | uspto-grants-1993_05 |
| ORD ID | ord-7dca0d1e7733477f968a6c1bcbc5a80b |
| 출처 메모 | uspto-grants-1993_05 |