참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Dodecanol | HCID 8193 | — |
| 반응물 | Ethyl mandelate | HCID 13050 | — |
| 생성물 | Lauryl mandelate | HCID 11587803 | 62.3% |
반응 단계
A mixture of Novozym® 435 (2.21 g), molecular sieves (18.60 g), 1-dodecanol (3.76 g), and ethyl mandelate (3.61 g) in a 150 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.0 g of lauryl mandelate (56% yield) was obtained as a clear viscous liquid. The purity of the product was >95% as assessed by HPLC-DAD.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07863025B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_01 |
|---|
| ORD ID | ord-e4f46e96d3414ea6b1ddb8db33c7ce15 |
|---|
| 출처 메모 | uspto-grants-2011_01 |
|---|
