Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → N-(3-formylphenyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | N-[3-(1,3-dioxolan-2-yl)phenyl]acetamide | HCID 13987600 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N-(3-formylphenyl)acetamide | HCID 256849 | 100.6% |
반응 단계
A solution of N-[3-(1,3-dioxolan-2-yl)phenyl]acetamide (50.0 g, 0.24 mole) and p-toluenesulfonic acid (1.0 g) in acetone (750 mL) was stirred at room temperature for 72 hours. The solution was filtered through a pad of neutral alumina and concentrated in vacuo to afford N-(3-formylphenyl)acetamide (39.4 g, 100%), mp 68°-70° C., used without further purification below.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04701459 |
| 출처 데이터셋 | uspto-grants-1987_10 |
| ORD ID | ord-2a1da0083d5e4beb8dfc71136665e958 |
| 출처 메모 | uspto-grants-1987_10 |